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Durham University

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Publication details for Prof. Ivana Evans

I. R. Evans, J. A. K. Howard, K. M. Szecsenyi, V. M. Leovac & Z. K. Jacimovic (2004). Synthesis, characterization and crystal structure of a novel Ni(II) complex, Ni(L-H)(2) (L=3,5-dimethyl-1-thiocarboxamidopyrazole). Journal of Coordination Chemistry 57(6): 469-476.
  • Publication type: Journal Article

Author(s) from Durham


A new complex, Ni(L-H)(2), L = 3,5-dimethyl-1-thiocarboxamidopyrazole, has been synthesized and characterized by IR spectroscopy, magnetic and electrical measurements. Its crystal structure was solved from powder X-ray diffraction data. The compound crystallizes in space group P (1) over bar with two independent half-molecules containing Ni(II) coordinated by four nitrogen atoms in a square-plane. The packing pattern consists of two stacks of parallel molecules mutually tilted at an angle of 118degrees.